Whiteboard Chemistry with Joe White

Thermodynamics

Lattice enthalpy and Born–Haber cycles, the perfect ionic model and covalent character, enthalpies of solution and hydration, entropy, and how Gibbs free energy decides whether a reaction is feasible.

AQA 7404/7405 Paper 1 A-level only
ΔH TΔS
Where this sits

Thermodynamics extends Energetics (3.1.4). Energetics measured enthalpy changes and used Hess’s law; thermodynamics uses the same cycle-building to reach quantities that cannot be measured directly — above all lattice enthalpy — and then adds a second idea, entropy, to answer a question enthalpy alone cannot: will a reaction actually happen? The whole topic is A-level only and rewards careful bookkeeping of signs and units.

Lattice enthalpy & the key definitions

An ionic lattice is held together by the electrostatic attraction between oppositely charged ions. The energy of that attraction is measured by the lattice enthalpy, which AQA defines in two equal-and-opposite ways. It is the number that puts a figure on the stability of an ionic compound: the more exothermic the lattice enthalpy of formation, the more strongly the ions are held and the more stable the solid.

Key definitions — lattice enthalpy

Lattice enthalpy of formation is the enthalpy change when one mole of a solid ionic compound is formed from its gaseous ions.

Lattice enthalpy of dissociation is the enthalpy change when one mole of a solid ionic compound is separated into its gaseous ions.

Forming a lattice releases energy, so lattice enthalpy of formation is exothermic (negative); pulling the lattice apart requires energy, so lattice enthalpy of dissociation is endothermic (positive). The two values are identical in size and opposite in sign. Lattice enthalpy cannot be measured directly — it is found using a Born–Haber cycle, which needs the five enthalpy terms below.

TermDefinition (enthalpy change when…)Sign
Enthalpy of formation, ΔfHone mole of a compound forms from its elements in their standard statesusually −
Enthalpy of atomisation, ΔatHone mole of gaseous atoms forms from an element in its standard state+
First ionisation energyone mole of electrons is removed from one mole of gaseous atoms (forming 1+ ions)+
Bond dissociation enthalpyone mole of a specified covalent bond is broken in gaseous molecules+
First electron affinityone mole of gaseous atoms gains one mole of electrons (forming 1− ions)
+ + + + NaCl(s) giant ionic lattice lattice dissociation ΔH = + endothermic lattice formation ΔH = − exothermic + + Cl⁻ Na⁺ Na⁺ Cl⁻ Na⁺(g) + Cl⁻(g) separated gaseous ions The two values are equal in size and opposite in sign.
Lattice enthalpy measures the strength of the ionic bonding. It is more exothermic for smaller, more highly charged ions.
Precision points
  • Every definition specifies one mole and the correct states (gaseous ions for lattice enthalpy and electron affinity). Omitting either loses the mark.
  • The first electron affinity is exothermic, but the second is endothermic: adding an electron to an already negative ion means bringing a negative charge towards a repelling negative ion.
  • Lattice enthalpy is more exothermic for ions that are smaller and more highly charged (greater charge density → stronger attraction).
Exam questions
Q1 [2 marks]

Define the term enthalpy of lattice dissociation.

Show answer

The enthalpy change when one mole of a solid ionic compound… 1 mark

…is separated (dissociates fully) into its gaseous ions. 1 mark

A suitable equation with state symbols for the ions is acceptable. Not “one mole of gaseous ions”.

Q2 [1 mark]

Explain why the second electron affinity of oxygen has a positive value.

Show answer

The electron is being added to an O ion, which repels the incoming (negative) electron, so energy must be supplied. 1 mark

Q3 [1 mark]

Explain why the second ionisation energy of calcium is greater than its first ionisation energy.

Show answer

The second electron is removed from a positive ion (Ca+): the same number of protons attract fewer electrons, so the remaining electrons are held more strongly (and the ion is smaller). 1 mark

Q4 [1 mark]

State the meaning of the term enthalpy change.

Show answer

A heat (energy) change measured at constant pressure. 1 mark

“Energy change” on its own is ignored — the constant-pressure condition is the mark. Conditions quoted alongside it are ignored even if wrong.

Q5[1 mark]

The enthalpies of lattice formation of MgCl2, MgO and BaCl2 are −2018, −2493 and −3889 kJ mol−1, in some order. Select the correct match. Tick (✓) one box.

Q6 [2 marks]

Explain why the enthalpy of lattice dissociation of sodium oxide is greater than the enthalpy of lattice dissociation of sodium chloride.

Show answer

The oxide ion has a higher (negative) charge than the chloride ion, and is smaller — so it has a higher charge density (higher charge : size ratio). 1 mark

There is therefore a stronger attraction between the oppositely charged ions (O2− and Na+), so more energy is needed to separate them. 1 mark

Ignore references to electronegativity.

Source: AQA A-Level Chemistry past papers.

Born–Haber cycles

A Born–Haber cycle is Hess’s law applied to the formation of an ionic solid. There are two routes from the elements in their standard states to the solid lattice: the direct route (enthalpy of formation), and the indirect route that goes up through gaseous atoms and gaseous ions and then down into the lattice. Because both routes have the same overall enthalpy change, you can find any missing step.

Rearrange to make the unknown the subject. Two things cause almost every lost mark: forgetting to multiply a step by the number of atoms or ions (two chlorides need 2 × atomisation and 2 × electron affinity), and mishandling a sign. Colour-code each step: energy in is positive, energy out is negative.

Worked example — lattice enthalpy of NaCl

Step 1 — write the cycle as a Hess relationship:

Step 2 — rearrange for the lattice enthalpy:

Step 3 — substitute (−411, +109, +494, +121, −364):

Born–Haber cycle for MgO(s) up = endothermic (+) down = exothermic (−) enthalpy Mg²⁺(g) + O²⁻(g) Mg²⁺(g) + 2e⁻ + O(g) Mg²⁺(g) + O⁻(g) + e⁻ Mg⁺(g) + e⁻ + O(g) Mg(g) + O(g) Mg(g) + ½O₂(g) Mg(s) + ½O₂(g) MgO(s) atomisation of Mg ½ × bond dissociation of O₂ 1st ionisation energy of Mg 2nd ionisation energy of Mg 1st electron affinity of O 2nd electron affinity of O endothermic — this step goes up lattice enthalpy of formation of MgO(s) direct route — ΔfH(MgO) = +150 ½(496) = +248 +736 +1450 −142 +844 −3888 −602 Levels are not to scale · all values in kJ mol⁻¹
Both routes to the lattice share the same enthalpy change, so any single step can be found from the others.
Exam questions
Q7 [3 marks]

Use the data below to calculate the enthalpy of lattice formation of magnesium oxide.

Enthalpy of formation of MgO−602
Enthalpy of atomisation of magnesium+150
First ionisation energy of magnesium+736
Second ionisation energy of magnesium+1450
Bond dissociation enthalpy of oxygen+496
First electron affinity of oxygen−142
Second electron affinity of oxygen+844

All values in kJ mol−1.

Show answer

ΔfH = ΔatH(Mg) + ½ BDE(O2) + IE1 + IE2 + EA1(O) + EA2(O) + ΔLEH 1 mark

−602 = 150 + (½ × 496) + 736 + 1450 + (−142) + 844 + ΔLEH 1 mark

ΔLEH(MgO) = −602 − 3286 = −3888 kJ mol−1 1 mark

Use only ½ of the O=O bond enthalpy (one O atom per MgO). +3888 scores 1 mark; missing the ½ gives −4136.

Q8 [2 marks]

A Born–Haber cycle for caesium iodide uses these data (all kJ mol−1): enthalpy of formation of CsI −337; enthalpy of atomisation of caesium +79; first ionisation energy of caesium +376; electron affinity of iodine −314; enthalpy of lattice formation of CsI −585. Calculate the standard enthalpy of atomisation of iodine.

Show answer

−337 = 79 + ΔatH(I) + 376 + (−314) + (−585) 1 mark

ΔatH(I) = −337 − (−444) = +107 kJ mol−1 1 mark

−107 scores 1 mark. Answer to 2 sig figs or more.

Q9 [2 marks]

A Born–Haber cycle for caesium iodide is built in this order: the elements in their standard states are atomised, caesium is then ionised, an electron is transferred to the gaseous iodine atom, and finally the gaseous ions come together to form the lattice. Write the formulae, including state symbols, of all the species present (a) on the lowest level of the cycle, the elements in their standard states, and (b) on the highest level of the cycle — reached after atomisation and ionisation, but before the electron affinity step.

Show answer

(a) Cs(s) + ½I2(s) 1 mark

(b) Cs+(g) + e + I(g) 1 mark

State symbols are required on every species. Iodine is a solid in its standard state, and only ½ mol of I2 is needed for one mole of CsI. The free electron must be shown on the upper level.

Q10 [3 marks]

A Born–Haber cycle for magnesium oxide starts from Mg(s) + ½O2(g) and finishes at MgO(s). Write the formulae, including state symbols, of all the species present on each of the three levels between them: (a) after both elements have been atomised; (b) after the first and second ionisation energies of magnesium have been supplied; (c) after the first and second electron affinities of oxygen, immediately before the lattice-formation step.

Show answer

(a) Mg(g) + O(g) 1 mark

(b) Mg2+(g) + 2e + O(g) 1 mark

(c) Mg2+(g) + O2−(g) 1 mark

One mark for each level, and only with correct state symbols. The two electrons released by magnesium must be shown on level (b), because they have not yet been transferred to oxygen.

Q11 [3 marks]

An incomplete Born–Haber cycle for the formation of calcium chloride has three blank levels: (a) the lowest level, the elements in their standard states; (b) the level reached once both ionisation energies of calcium have been supplied, before the chlorine has been atomised; (c) the level of gaseous ions immediately before the lattice-formation step down to CaCl2(s). Write the formulae, including state symbols, of all the species on each level.

Show answer

(a) Ca(s) + Cl2(g) 1 mark

(b) Ca2+(g) + 2e + Cl2(g) 1 mark

(c) Ca2+(g) + 2Cl(g) 1 mark

For (b) the alternative Ca+(g) + e + 2Cl(g) is also allowed. Note that two chloride ions are needed on level (c).

Q12 [2 marks]

A different Born–Haber cycle for calcium chloride atomises the chlorine before the electron transfer. Two levels are blank: (i) the level reached once calcium has been fully ionised and the chlorine fully atomised, before the electron affinity step; (ii) the level of gaseous ions immediately before the lattice-formation step. Write the formulae of the missing species on each of these two levels.

Show answer

(i) Ca2+(g) + 2e + 2Cl(g) 1 mark

(ii) Ca2+(g) + 2Cl(g) 1 mark

Every ×2 must be shown: two chlorine atoms, then two chloride ions, and two electrons released by the calcium.

Q13 [2 marks]

Use the cycle in part (a) and the data below to calculate the second ionisation energy of calcium.

Enthalpy of atomisation of calcium+193
First ionisation energy of calcium+590
Enthalpy of atomisation of chlorine+121
Electron affinity of chlorine−364
Enthalpy of formation of calcium chloride−795
Enthalpy of lattice formation of calcium chloride−2237

All values in kJ mol−1.

Show answer

−795 = 193 + 590 + IE2 + (2 × 121) + (2 × −364) + (−2237) 1 mark

The known terms sum to −1940, so −795 = −1940 + IE2

IE2(Ca) = −795 + 1940 = +1145 kJ mol−1 1 mark

Setting out the first line as −795 = −1940 + IE2 also earns the first mark. Both ×2 factors are needed — one on atomisation of chlorine and one on the electron affinity.

Q14 [3 marks]

Use the data below, from a Born–Haber cycle for strontium chloride (SrCl2), to calculate a value for the electron affinity of chlorine.

Enthalpy of atomisation of strontium+164
First ionisation energy of strontium+548
Second ionisation energy of strontium+1060
Enthalpy of atomisation of chlorine+121
Enthalpy of formation of strontium chloride−828
Enthalpy of lattice formation of strontium chloride−2112

All values in kJ mol−1.

Show answer

−828 = 164 + (2 × 121) + 548 + 1060 + (2 × EA) + (−2112) 1 mark

The known terms sum to −98, so 2 × EA = −828 + 98 = −730 1 mark

EA(Cl) = −730 ÷ 2 = −365 kJ mol−1 1 mark

Two chlorides mean a ×2 on atomisation and on the electron affinity — and then the final answer must be halved back to a per-ion value. Answers of +365, −304.5 or −730 score 2 of the 3 marks; +304.5, +730 or −609 score 1; +609 scores 0.

Q15 [2 marks]

Use the data below to calculate the enthalpy of lattice dissociation of sodium oxide, Na2O.

Enthalpy of atomisation of oxygen+248
Enthalpy of atomisation of sodium+109
Enthalpy of formation of sodium oxide−416
First ionisation energy of sodium+494
First electron affinity of oxygen−142
Second electron affinity of oxygen+844

All values in kJ mol−1.

Show answer

−416 + ΔLEH(dissociation) = 248 + (2 × 109) + (2 × 494) + (−142) + 844 = 2156 1 mark

ΔLEH(dissociation) = 2156 + 416 = +2572 kJ mol−1 1 mark

−2572 scores 1 mark. Two ×2 factors are needed here (two sodium atoms are atomised and two are ionised), and both electron affinities of oxygen are used. The enthalpy of atomisation of oxygen is given directly, so there is no ½ factor — that only appears when the bond dissociation enthalpy of O2 is supplied instead.

Q16 [2 marks]

Use the data below to calculate a value for the enthalpy of lattice dissociation of calcium chloride.

Enthalpy of formation of calcium chloride−795
Enthalpy of atomisation of calcium+193
First ionisation energy of calcium+590
Second ionisation energy of calcium+1150
Enthalpy of atomisation of chlorine+121
Electron affinity of chlorine−364

All values in kJ mol−1.

Show answer

−795 + ΔLEH(dissociation) = 193 + 590 + 1150 + (2 × 121) + (2 × −364) = 1447 1 mark

ΔLEH(dissociation) = 1447 + 795 = +2242 kJ mol−1 1 mark

−2242 scores 1 mark. If one or both of the ×2 factors is missing the answer comes out as +2485, +2121 or +2606 — each worth 1 mark.

Source: AQA A-Level Chemistry past papers.

The perfect ionic model & covalent character

Lattice enthalpy can also be calculated theoretically from a model of the crystal. That model makes a simplifying assumption.

Key definition

The perfect ionic model treats the ions as point charges (perfect, undistorted spheres) with no covalent character.

Comparing the theoretical value with the experimental value from a Born–Haber cycle tests how well that assumption holds:

  • If the two values are close, the compound is close to purely ionic — the perfect ionic model works well.
  • If the experimental value is significantly more exothermic than the theoretical value, there is additional covalent character: the cation polarises (distorts) the anion’s electron cloud, so the electrons are partly shared and the bonding is stronger than the ionic model predicts.

Covalent character is greatest when the cation is small and highly charged (high polarising power) and the anion is large (easily polarised).

Perfect ionic model Na⁺ Cl⁻ perfect undistorted spheres point charges from the centre theoretical ≈ experimental lattice enthalpy Polarised — covalent character I⁻ Al³⁺ shared electron density the anion’s cloud is pulled over electron density shared in the gap experimental more exothermic than theoretical
A big gap between the theoretical and experimental lattice enthalpy is evidence of covalent character.
Exam questions
Q17 [1 mark]

The experimental lattice enthalpy of caesium iodide is −585 kJ mol−1; the value from the perfect ionic model is −582 kJ mol−1. Deduce what these values indicate about the bonding in caesium iodide.

Show answer

The values are very close, so caesium iodide is almost purely (perfectly) ionic, with little or no covalent character. 1 mark

Penalise references to atoms or molecules; the species are ions.

Q18 [1 mark]

For silver chloride the theoretical lattice enthalpy is −770 kJ mol−1 and the experimental value is −905 kJ mol−1. State why there is a difference between these values.

Show answer

Silver chloride has covalent character (partial covalent bonding): the Ag+ ion polarises / distorts the chloride ion. 1 mark

Q19 [1 mark]

Theoretical values for enthalpies of lattice dissociation can be calculated using a perfect ionic model. State the meaning of the term perfect ionic model.

Show answer

The ions are treated as point charges (perfect spheres) with no covalent character — there is no polarisation of the ions. 1 mark

Do not use the words “atoms” or “molecules” anywhere in this answer — the species are ions.

Source: AQA A-Level Chemistry past papers.

Enthalpies of solution & hydration

When an ionic solid dissolves, the lattice must break apart and the freed ions become surrounded by water molecules. A Hess cycle links the two.

Key definitions

Enthalpy of hydration is the enthalpy change when one mole of gaseous ions is dissolved in water to form one mole of aqueous ions.

Enthalpy of solution is the enthalpy change when one mole of an ionic solid dissolves completely in water to form a very dilute solution.

The dissolving cycle breaks the solid into gaseous ions (lattice dissociation, endothermic) and then hydrates them (exothermic):

Worked example — enthalpy of solution of NaCl

Lattice dissociation of NaCl = +771; hydration of Na+ = −406; hydration of Cl = −364 (kJ mol−1).

Hydration is more exothermic for ions with a higher charge density — smaller ions and more highly charged ions attract the polar water molecules (the Oδ− or Hδ+) more strongly.

NaCl(s) Na+(g) + Cl(g) Na+(aq) + Cl(aq) lattice dissociation enthalpy ΔLEH = +771 hydration — ΣΔhydH (−406) + (−364) = −770 enthalpy of solution ΔsolH = +1 ΔsolH = ΔLEH + ΣΔhydH = +771 + (−770) = +1 Hydration, close up each water turns its O end to the ion O O O O H H H H H H H H δ δ δ δ δ+ δ+ δ+ δ+ δ+ δ+ δ+ δ+ Na+
Enthalpy of solution is the small difference between two large numbers — so a sign slip changes the answer completely.
Exam questions
Q20 [3 marks]

Use the data to calculate the molar enthalpy change when calcium chloride dissolves in water, then deduce how the temperature changes. Hydration of Ca2+ = −1650; hydration of Cl = −364; lattice formation of CaCl2 = −2237 (kJ mol−1).

Show answer

ΔsolH = ΔLEH(dissociation) + ΔhydH(Ca2+) + 2ΔhydH(Cl) = (+2237) + (−1650) + (2 × −364) 1 mark

ΔsolH = −141 kJ mol−1 1 mark

The value is negative (exothermic), so the temperature rises. 1 mark

Lattice dissociation = −(lattice formation) = +2237. Remember the ×2 for two chloride ions.

Q21 [3 marks]

Calcium bromide dissolves in water. Using enthalpy of solution of CaBr2 = −110, lattice formation of CaBr2 = −2176 and hydration of Ca2+ = −1650 (kJ mol−1), calculate the enthalpy of hydration of bromide ions.

Show answer

−110 = (+2176) + (−1650) + 2ΔhydH(Br) 1 mark

hydH(Br) = −636 1 mark

ΔhydH(Br) = −318 kJ mol−1 1 mark

Q22 [2 marks]

Explain why the enthalpy of hydration of fluoride ions is more exothermic than that of chloride ions.

Show answer

The fluoride ion is smaller, so it has a higher charge density. 1 mark

This gives a stronger attraction between the ion and the Hδ+ of the water molecules. 1 mark

Do not accept “fluorine atoms are smaller” or references to ionic bonds.

Q23 [1 mark]

Magnesium chloride dissolves in water. Give an equation, including state symbols, to represent the process that occurs when the enthalpy of solution of magnesium chloride is measured.

Show answer

MgCl2(s) → Mg2+(aq) + 2Cl(aq) 1 mark

⇌ is allowed in place of →, and “+ aq” may be written on the left-hand side. The ×2 on the chloride ion is required.

Q24 [3 marks]

The enthalpy of solution of ammonium nitrate is the enthalpy change for NH4NO3(s) + aq → NH4+(aq) + NO3(aq), ΔH = +26 kJ mol−1. The enthalpies of hydration are −307 kJ mol−1 for NH4+(g) and −314 kJ mol−1 for NO3(g). Write the Hess relationship that links these three quantities, naming the species at each corner of the cycle, and use it to calculate the enthalpy of lattice dissociation of ammonium nitrate.

Show answer

The cycle has three corners — NH4NO3(s), the gaseous ions NH4+(g) + NO3(g), and the aqueous ions NH4+(aq) + NO3(aq) — so ΔsolH = ΔLEH(dissociation) + ΔhydH(NH4+) + ΔhydH(NO3) 1 mark

26 = ΔLEH(dissociation) + (−307) + (−314), so ΔLEH(dissociation) = 26 + 307 + 314 1 mark

ΔLEH(dissociation) = +647 kJ mol−1 1 mark

In the original question the first mark was for drawing the labelled cycle itself — three corners with formulae, state symbols and arrows. An equivalent Born–Haber-style energy cycle is accepted. Answers of −647 or ±595 score 2 of the 3 marks.

Q25 [3 marks]

A student measures 25.0 cm3 of distilled water into a beaker, records its temperature, adds 4.00 g of solid NH4NO3, stirs, and records the lowest temperature reached. The initial temperature is 20.2 °C and the lowest temperature is 12.2 °C. Calculate the enthalpy of solution, in kJ mol−1, for ammonium nitrate in this experiment. Assume the specific heat capacity of the solution c = 4.18 J K−1 g−1 and the density of the solution = 1.00 g cm−3. Mr(NH4NO3) = 80.0.

Show answer

q = mcΔT = 25.0 × 4.18 × (20.2 − 12.2) = 25.0 × 4.18 × 8.0 = 836 J 1 mark

n(NH4NO3) = 4.00 ÷ 80.0 = 0.0500 mol 1 mark

ΔsolH = 836 ÷ 0.0500 = 16 720 J mol−1 = +16.7 kJ mol−1 1 mark

Use the mass of water, 25.0 g — using m = 29 g is not allowed and gives +19.4 (2 of 3 marks). The temperature fell, so the change is endothermic and the answer is positive; −16.7 scores 2 of 3. Two significant figures or more.

Q26 [1 mark]

The uncertainty in each of the temperature readings from the thermometer used in this experiment is ±0.1 °C. Calculate the percentage uncertainty in the temperature change.

Show answer

(2 × 0.1 ÷ 8.0) × 100 = 2.5% 1 mark

Two readings are taken to find one temperature change, so the ±0.1 °C uncertainty is counted twice.

Q27 [2 marks]

Suggest a change to the student’s method, using the same apparatus, that would reduce the percentage uncertainty in the temperature change. Give a reason for your answer.

Show answer

Change: use a larger mass of NH4NO3 (or a smaller volume of water). 1 mark

Reason: the temperature change is then greater (the final temperature is lower), so the same ±0.1 °C is a smaller percentage of it. 1 mark

The two marking points are independent. “Larger volume of water” and “final temperature is higher” are not accepted; higher concentration, and any change of apparatus such as adding insulation, are ignored.

Q28 [1 mark]

Another student obtained a value of +15 kJ mol−1 using the same method. Suggest the main reason for the difference between this experimental value and the correct value of +26 kJ mol−1.

Show answer

Heat was gained from the surroundings (or the solid did not dissolve completely). 1 mark

“Heat loss” is not accepted. The change is endothermic, so the beaker is colder than its surroundings and thermal energy flows in, making the measured temperature drop too small. References to mistakes in the method are ignored.

Q29 [2 marks]

The enthalpies of hydration of Li+(g), Na+(g) and K+(g) are −519, −406 and −322 kJ mol−1 respectively. Explain why the enthalpy of hydration becomes less exothermic from Li+ to K+.

Show answer

From Li+ to K+ the size of the ion increases (more shells, larger ionic radius), so the charge density decreases. 1 mark

The electrostatic attraction between the metal ion and the Oδ− of the water molecules is therefore weaker. 1 mark

Do not write “atomic radius” or refer to molecules — these are ions. The second mark does not depend on the first, and converse arguments are accepted. Note that a cation is attracted to the Oδ− end of water, whereas an anion is attracted to the Hδ+ end.

Q30 [1 mark]

Give a reason why data books do not contain a value for the enthalpy of solution of sodium oxide.

Show answer

Sodium oxide reacts with water (to form a solution of NaOH) rather than simply dissolving. 1 mark

“It dissolves in water” is not accepted — the answer must say that a reaction occurs.

Source: AQA A-Level Chemistry past papers.

Entropy, ΔS

Enthalpy alone cannot explain why some endothermic reactions still happen. The missing idea is entropy, S — a measure of how disordered a system is, or how many ways its particles and energy can be arranged. Nature tends towards greater disorder.

Entropy rises as particles gain freedom of movement, so solid < liquid < gas. It also increases when a solid dissolves and when a reaction produces more moles of gas. A perfect crystal at 0 K has zero entropy.

entropy, S, increases solid liquid gas regular lattice, touching still touching, disordered far apart, random H2O(s) H2O(l) H2O(g) 48 70 189 S in J K−1 mol−1 a perfect crystal at 0 K has S = 0 only 6 gas particles are drawn — at this spacing the rest lie beyond the frame
The state and number of gas moles are the quickest guide to the sign of ΔS.

Calculate an entropy change as products minus reactants, using absolute entropy values (in J K−1 mol−1):

Exam questions
Q31 [2 marks]

Calculate the entropy change for the reaction 4NH3(g) + 5O2(g) ⇌ 4NO(g) + 6H2O(g). Standard entropies (J K−1 mol−1): NH3 193, O2 205, NO 211, H2O 189.

Show answer

ΔS = [(4 × 211) + (6 × 189)] − [(4 × 193) + (5 × 205)] = 1978 − 1797 1 mark

ΔS = +181 J K−1 mol−1 1 mark

Q32 [2 marks]

(a) Explain why the standard entropy of carbon dioxide is greater than that of carbon. (b) State the temperature at which the standard entropy of solid aluminium is 0 J K−1 mol−1.

Show answer

(a) Carbon dioxide is a gas, so it is more disordered than solid carbon. 1 mark

(b) 0 K (absolute zero / −273 °C). 1 mark

Source: AQA A-Level Chemistry past papers.

Gibbs free energy & feasibility

Enthalpy and entropy are combined in the Gibbs free-energy change, which decides whether a reaction is thermodynamically feasible (able to happen):

T is the temperature in kelvin. A reaction is feasible when ΔG is zero or negative. A units mismatch is easy to make here, because ΔH is quoted in kJ mol−1 but ΔS in J K−1 mol−1.

Precision points
  • Convert ΔS to kJ (divide by 1000) before substituting, or the TΔS term is a thousand times too big. Entropy is almost always given in joules.
  • Consider a reaction with ΔH = +30 kJ mol−1 and ΔS = +50 J K−1 mol−1 at 298 K. Correctly, ΔG = 30 − 298 × 0.050 = +15 kJ mol−1 (not feasible). Forget to convert and you get 30 − 298 × 50 = −14 870, wrongly “feasible”.
  • Give the answer to 3 significant figures and keep the minus sign on exothermic values.

Because ΔG = ΔH − TΔS, temperature matters. The reaction is on the boundary of feasibility when ΔG = 0, which rearranges to give the temperature at which it just becomes feasible:

Plotting ΔG against T gives a straight line: the intercept is ΔH and the gradient is −ΔS.

ΔG / kJ mol−1 100 50 0 −50 145 ΔG = 0 not feasible (ΔG > 0) ΔG ≤ 0 — feasible feasible only above 853 K ΔT = 400 K −68 kJ mol−1 intercept = ΔH = +145 kJ mol−1 gradient = −ΔS = −0.170 kJ K−1 mol−1 0 200 400 600 800 1000 1200 temperature, T / K T = ΔH / ΔS = 145 / 0.170 ≈ 853 K
The intercept gives ΔH and the gradient gives −ΔS, so both can be read straight off a ΔG–T line.
Exam questions
Q33 [6 marks]

For CO2(g) + 3H2(g) ⇌ CH3OH(g) + H2O(g), calculate ΔG at 890 K. Data: ΔfH / kJ mol−1: CO2 −394, H2 0, CH3OH −201, H2O −242. S / J K−1 mol−1: CO2 214, H2 131, CH3OH 238, H2O 189.

Show answer

ΔH = [(−201) + (−242)] − [(−394) + 0] = −49 kJ mol−1 1 mark

ΔS = [238 + 189] − [214 + (3 × 131)] = 427 − 607 = −180 J K−1 mol−1 1 mark

ΔG = ΔH − TΔS 1 mark

Convert ΔS: −180 J = −0.180 kJ K−1 mol−1 1 mark

ΔG = −49 − (890 × −0.180) = −49 + 160 1 mark

ΔG = +111 kJ mol−1 1 mark

Leaving ΔS in J gives +160 151 — the classic unit error.

Q34 [3 marks]

For a gas-phase reaction, a straight-line graph of ΔG against T has a y-intercept of +145 kJ mol−1 and a gradient of −0.170 kJ K−1 mol−1. Deduce ΔH and ΔS, and state the temperature above which the reaction is feasible.

Show answer

ΔH = intercept = +145 kJ mol−1. 1 mark

Gradient = −ΔS, so ΔS = +0.170 kJ K−1 mol−1 = +170 J K−1 mol−1. 1 mark

Feasible when ΔG ≤ 0: T = ΔH / ΔS = 145 / 0.170 ≈ 853 K, so feasible above about 850 K. 1 mark

Q35 [5 marks]

For 2Al2O3(s) + 3C(s) → 4Al(s) + 3CO2(g), calculate the minimum temperature at which the reaction becomes feasible. Data: ΔfH / kJ mol−1: Al2O3 −1669, Al 0, C 0, CO2 −394. S / J K−1 mol−1: Al2O3 51, Al 28, C 6, CO2 214.

Show answer

ΔH = [3 × (−394)] − [2 × (−1669)] = −1182 + 3338 = +2156 kJ mol−1 1 mark

ΔS = [(4 × 28) + (3 × 214)] − [(2 × 51) + (3 × 6)] = 754 − 120 = +634 J K−1 mol−1 1 mark

At the boundary ΔG = 0, so T = ΔH / ΔS 1 mark

Convert ΔS: +634 J = +0.634 kJ K−1 mol−1 1 mark

T = 2156 / 0.634 = 3400 K (to 3 s.f.) 1 mark

The reaction is endothermic with a positive ΔS, so it becomes feasible only above this temperature.

Q36 [2 marks]

For 4NH3(g) + 5O2(g) ⇌ 4NO(g) + 6H2O(g), ΔH = −905 kJ mol−1 and ΔS = +181 J K−1 mol−1. Calculate a value for the Gibbs free-energy change (ΔG), in kJ mol−1, at 600 °C.

Show answer

ΔG = ΔH − TΔS = −905 − [(600 + 273) × 181 × 10−3] 1 mark

ΔG = −905 − 158 = −1063 kJ mol−1 1 mark

Allow −1060. T must be converted to kelvin: 600 °C = 873 K. Using 600 K instead loses the mark.

Q37 [2 marks]

The reaction between ammonia and oxygen was then carried out at a higher temperature. Explain how this change affects the value of ΔG for the reaction.

Show answer

ΔG becomes more negative (less positive). 1 mark

ΔS is positive, so raising T makes TΔS bigger, and −TΔS more negative. 1 mark

“ΔG increases / decreases / gets larger / gets smaller” on its own is ignored — say more negative or less positive.

Q38 [4 marks]

The enthalpy of formation of caesium iodide is −337 kJ mol−1. Use the entropy data below to show that the reaction CsI(s) → Cs(s) + ½I2(s) is not feasible at 298 K.

CsI(s)Cs(s)I2(s)
S / J K−1 mol−113082.8117
Show answer

ΔS = [82.8 + (½ × 117)] − 130 = 141.3 − 130 = +11.3 J K−1 mol−1 1 mark

ΔG = ΔH − TΔS, and this reaction is the reverse of the formation of CsI, so ΔH = +337 kJ mol−1 1 mark

ΔG = 337 − (298 × 11.3 × 10−3) = 337 − 3.37 1 mark

ΔG = +334 kJ mol−1 — positive, so the reaction is not feasible at 298 K. 1 mark

Any negative answer loses the final mark. The third mark is specifically for the unit conversion — ΔS into kJ K−1 mol−1 or ΔH into J mol−1. Note the ½ on the entropy of I2(s), matching the equation.

Q39 [4 marks]

Ammonium nitrate dissolves as NH4NO3(s) + aq → NH4+(aq) + NO3(aq), ΔH = +26 kJ mol−1. Using the entropy data below, calculate ΔG at 298 K and explain what your value indicates about the feasibility of this reaction. Assume that for the solvent, water, the entropy change ΔS = 0.

NH4NO3(s)151
NH4+(aq)113
NO3(aq)146

All entropies in J K−1 mol−1.

Show answer

ΔS = (113 + 146) − 151 = +108 J K−1 mol−1 1 mark

ΔG = ΔH − TΔS = 26 − (298 × 108 × 10−3) = 26 − 32.2 1 mark

ΔG = −6.18 kJ mol−1 1 mark

ΔG is negative, so the reaction is feasible (spontaneous) at 298 K. 1 mark

Allow −6.184 or −6.2. The final mark stands alone. This is the case worth remembering: the change is endothermicH positive), yet it is still feasible because the positive entropy change makes TΔS larger than ΔH.

Q40 [3 marks]

Calculate the temperature, in °C, at which the reaction NaCl(s) → Na(s) + ½Cl2(g) becomes feasible. ΔH = +411 kJ mol−1 and ΔS = +90.1 J K−1 mol−1.

Show answer

At the boundary ΔG = 0, so T = ΔH ÷ ΔS 1 mark

T = 411 ÷ (90.1 × 10−3) = 4562 K 1 mark

Temperature = 4562 − 273 = +4289 °C 1 mark

Allow 4290 °C. The question asks for degrees Celsius, so the −273 conversion carries the final mark on its own — stopping at 4562 K scores 2 of 3.

Source: AQA A-Level Chemistry past papers.

The thermodynamics checklist

On this topic the chemistry is rarely the hard part — the signs, units and × factors are. Working every calculation the same way keeps those under control.

The four-step checklist
  • Convert units first — entropy from J to kJ if enthalpy is in kJ.
  • Substitute carefully, keeping every sign and every × factor.
  • Evaluate the sign of the answer — and sanity-check it (exothermic should be negative).
  • Interpret: is ΔG ≤ 0 (feasible)? Then give the answer to 3 significant figures with units.
Precision points
  • Examiner reports identify three preventable losses on this topic: mixing entropy in joules with enthalpy in kilojoules, dropping the minus sign on an exothermic value, and not giving three significant figures.
  • In Born–Haber work the same care applies: every ×2 (for two ions) and every sign must be right, and lattice enthalpies of formation and dissociation differ only by sign.
Capstone question
Q41 [6 marks]

The table gives lattice enthalpies of dissociation (kJ mol−1) from the perfect ionic model and from Born–Haber cycles. Discuss the values: compare the three perfect-ionic values, then compare each perfect-ionic value with its Born–Haber value. Marked by levels of response.

Perfect ionic modelBorn–Haber cycle
Calcium chloride22232237
Potassium chloride690701
Silver chloride770905
Show answer

Comparing the perfect-ionic values: CaCl2 is much larger than KCl and AgCl because Ca2+ has a higher charge (and is a small ion), giving stronger attraction between the oppositely charged ions. Stage 1

Where the two methods agree: CaCl2 and KCl have very similar perfect-ionic and Born–Haber values, so their bonding is close to perfectly ionic (the ions behave as spherical point charges). Stage 2

Where they differ: AgCl shows a large difference (770 vs 905), so it has significant covalent character — the Ag+ ion is polarising and distorts the chloride ion’s electron cloud. Stage 3

Source: AQA A-Level Chemistry past papers.

3.1.8 Thermodynamics — Quick-reference summary
  • Lattice enthalpy: formation (gaseous ions → solid) is exothermic; dissociation (solid → gaseous ions) is endothermic; equal and opposite. More exothermic for smaller, higher-charge ions.
  • Born–Haber cycle = Hess’s law for ion formation: ΔfH = (atomisation + ionisation + bond + electron affinity terms) + lattice enthalpy of formation. Watch × factors and signs.
  • Perfect ionic model treats ions as point charges / perfect spheres. A large gap between the theoretical and Born–Haber (experimental) value indicates covalent character (the cation polarises the anion).
  • Enthalpy of solution = ΔLE(dissociation) + ΣΔhydH. Enthalpy of hydration is more exothermic for smaller, higher-charge ions.
  • Entropy ΔS = ΣS(products) − ΣS(reactants), in J K−1 mol−1. Disorder rises solid < liquid < gas.
  • Feasibility: ΔG = ΔH − TΔS; a reaction is feasible when ΔG ≤ 0. At the boundary ΔG = 0, so T = ΔH / ΔS. Convert ΔS to kJ before substituting.

Found an error or have a suggestion?

Help improve these notes by sending feedback.

Want to go deeper?

1-to-1 tuition led by a current AQA examiner.

Thermodynamics marks are won and lost on housekeeping: the right sign on every Born–Haber step, converting entropy from joules to kilojoules, and giving three significant figures. Sessions drill the cycles and feasibility calculations on real AQA past questions.

Enquire now
Ready to get started? Enquire now →