Whiteboard Chemistry with Joe White

Group 7 — the halogens

The trends in electronegativity and boiling point, the oxidising power of the halogens and reducing power of the halides, the silver nitrate test, and the disproportionation reactions of chlorine.

AQA 7404/7405 Paper 1
F₂Cl₂Br₂I₂ boiling point ↑ electronegativity ↓ GROUP 7
Building on GCSE

At GCSE you learned that the halogens get less reactive down the group and that a more reactive halogen displaces a less reactive one from its salt. A-Level explains why — through electronegativity, oxidising power and the reducing power of the halide ions — and adds the reactions with concentrated sulfuric acid, the silver nitrate test, and the disproportionation chemistry of chlorine.

The halogens are reactive non-metals that exist as diatomic molecules (F2, Cl2, Br2, I2). Two physical trends are examined, and they run in opposite directions.

The two trends, F → I

Electronegativity decreases down the group. The atoms get larger with more shells, so the shared (bonding) pair of electrons is further from the nucleus and more shielded — the nucleus attracts it less strongly.

Boiling point increases down the group. The molecules gain more electrons, so the van der Waals forces between molecules get stronger and more energy is needed to separate them — F2 and Cl2 are gases, Br2 a liquid, I2 a solid.

Bigger atoms, weaker pull on the bonding pair (electronegativity falls); bigger molecules, stronger van der Waals forces (boiling point rises).
Group 7 at room temperature — state & colour F₂ Fluorine GAS pale yellow Cl₂ Chlorine GAS yellow-green Br₂ Bromine LIQUID orange-brown I₂ Iodine SOLID grey-black DOWN GROUP 7 MELTING & BOILING POINT INCREASES RELATIVE MOLECULAR MASS INCREASES
Down the group the halogens go from gases (F2, Cl2) through a liquid (Br2) to a solid (I2): as the molecules get larger, the van der Waals forces between them strengthen and the boiling point rises.
Precision points
  • Electronegativity is about the bonding pair. Explain the fall with larger atoms / more shielding → weaker attraction for the shared pair of electrons, not the “outer electrons”.
  • Boiling point rises because of van der Waals forces between molecules — more electrons make them stronger. You are not breaking the covalent bonds inside X2.

Oxidising power & displacement

Halogens react by gaining an electron each to become halide ions — that makes them oxidising agents. How readily they do it decreases down the group: for the same reason electronegativity falls, a larger, more shielded atom attracts the incoming electron less strongly.

You see this ranking in displacement reactions: a halogen will displace the halide ions of any halogen below it, but not above. So chlorine displaces bromide and iodide; bromine displaces iodide; iodine displaces neither.

Cl2 + 2Br → 2Cl + Br2  (chlorine oxidises bromide; the solution turns orange)

In oxidation-number terms, chlorine is reduced (Cl 0 → −1) and the bromide is oxidised (Br −1 → 0) — the same bookkeeping you apply to the concentrated sulfuric acid and disproportionation reactions below.

Cl⁻(aq)Br⁻(aq)I⁻(aq) HALIDE SOLUTION + Cl₂+ Br₂+ I₂ ✓ orange soln Br₂ displaced ✓ brown soln I₂ displaced ✓ brown soln I₂ displaced ✓ displacement (new colour)   ✗ no reaction   — own halide, no change oxidising power ↓
Only the halide of a less reactive halogen is displaced. The new solution colour — orange Br2, brown I2 — is the evidence.
Precision points
  • Say what is oxidised. Not “chlorine oxidises” alone — chlorine oxidises the bromide ions (removes electrons from them) and is itself reduced.
  • Get the colours right. Displaced Br2 is an orange solution; displaced I2 is a brown solution / grey-black solid. Examiner reports flag wrong colours and products.
  • A halogen cannot displace one above it — oxidising power falls down the group, so iodine cannot displace bromide or chloride.
🧪 Exam-style questions
Q1 [1 mark]

Which equation shows a redox reaction that does not occur? Tick (✓) one box.

Q2 [1 mark]

Which pair of solutions, when mixed, reacts to form a dark brown solution? Tick (✓) one box.

Q3 [1 mark]

Which is a correct trend down Group 7 from fluorine to iodine? Tick (✓) one box.

Source: AQA A-Level Chemistry past papers.

Reducing power & conc. sulfuric acid

Turn it around and look at the halide ions. A halide reacts by losing its extra electron, acting as a reducing agent — and this gets easier down the group, because the outer electron of the bigger ion is held less tightly. Iodide is the strongest reducer.

The test bench for this is the reaction of solid sodium halides with concentrated sulfuric acid. All three first make the hydrogen halide, but the more strongly reducing halides then go on to reduce the sulfur in H2SO4 — further and further down the group.

Sodium halide + conc. H2SO4ProductsSulfur changeObservations
NaClNaHSO4 + HCl onlyno redoxmisty white fumes of HCl
NaBr+ Br2 + SO2S +6 → +4orange/brown fumes (Br2), choking SO2
NaI+ I2 + SO2 + S + H2SS +6 → −2grey-black I2, yellow S, rotten-egg H2S
SOLID SODIUM HALIDE + CONCENTRATED H₂SO₄ NaCl misty whitefumes of HCl no sulfur gas no redox S stays +6 Cl⁻ too weak to reduce S NaBr orange-brown Br₂+ choking SO₂ Br₂ + SO₂ Br⁻ reduces S S +6 → +4 (in SO₂) NaI grey-black I₂+ SO₂ + yellow S + rotten-egg H₂S I₂ + SO₂ + S + H₂S I⁻ reduces S fully S +6 → −2 (in H₂S) reducing power of the halide ion increases — the sulfur is reduced further
The further down the group, the stronger the reducer — so the sulfur is dragged from +6 all the way to −2 (H2S) with iodide.
The equations

NaCl — acid–base only; chloride is too weak to reduce the sulfur:

NaCl + H2SO4 → NaHSO4 + HCl

NaBr — the acid–base step first (as for every sodium halide), then the HBr reduces the sulfur to SO2:

NaBr + H2SO4 → NaHSO4 + HBr

2HBr + H2SO4 → Br2 + SO2 + 2H2O   (S: +6 → +4)

NaI — the acid–base step first, then the HI reduces the sulfur further and further, giving three different sulfur products:

NaI + H2SO4 → NaHSO4 + HI

2HI + H2SO4 → I2 + SO2 + 2H2O   (S: +6 → +4)

6HI + H2SO4 → 3I2 + S + 4H2O   (S: +6 → 0)

8HI + H2SO4 → 4I2 + H2S + 4H2O   (S: +6 → −2)

Precision points
  • NaCl is the odd one out — it makes HCl only and produces no sulfur-containing gas, because chloride is too weak to reduce the sulfur.
  • H2S (rotten eggs) is the give-away for iodide; SO2 (choking) appears with bromide. Match the gas to the halide.
  • Check the equation type. Examiner reports flag full, ionic and half-equations being muddled — give exactly what is asked for.
🧪 Exam-style questions
Q1 [1 mark]

Some solid sodium halides are reacted with concentrated sulfuric acid. Which solid sodium halide does not produce a sulfur-containing gas as one of the products? Tick (✓) one box.

Q2 [1 mark]

Which statement is correct? Tick (✓) one box.

Q3 [3 marks]

Concentrated sulfuric acid oxidises iodide ions, and is itself reduced to H2S. Give the two half-equations and the overall ionic equation for this reaction.

Show answer

Oxidation: 2I → I2 + 2e 1 mark

Reduction: H2SO4 + 8H+ + 8e → H2S + 4H2O 1 mark

Overall: H2SO4 + 8H+ + 8I → 4I2 + H2S + 4H2O 1 mark

Scale the iodide half-equation by 4 so its 8 electrons match the reduction, then add and cancel.

Source: AQA A-Level Chemistry past papers.

The halide test & Required Practical 4

To identify a halide ion in solution, add dilute nitric acid, then silver nitrate solution. Silver ions give an insoluble silver halide whose colour names the ion:

HalideWith acidified AgNO3In ammonia
Fno precipitate (AgF is soluble)
Clwhite AgCl precipitatedissolves in dilute ammonia
Brcream AgBr precipitatedissolves in concentrated ammonia
Iyellow AgI precipitateinsoluble, even in concentrated ammonia

Ag+(aq) + Cl(aq) → AgCl(s)

AgCl(s) + 2NH3(aq) → [Ag(NH3)2]+(aq) + Cl(aq)

Three “why” questions are examined together: silver nitrate is used because Ag+ forms an insoluble silver halide; it is acidified with nitric acid to remove carbonate and hydroxide ions that would also give a precipitate (a false positive); and ammonia is added to tell the silver halide precipitates apart by their different solubilities — the surest way to separate white AgCl from cream AgBr.

ADD DILUTE HNO₃, THEN AgNO₃(aq) AgCl · white dissolves indilute NH₃ AgBr · cream dissolves only inconcentrated NH₃ AgI · yellow insoluble, even inconcentrated NH₃ acidify with dilute HNO₃ first — never HCl (adds Cl⁻) or H₂SO₄ (adds SO₄²⁻), which would give false precipitates
The colour narrows it down; ammonia settles a close call between a white and a cream precipitate.
Required practical 4 — testing for ions

RP4 is a set of test-tube reactions to identify cations (Group 2 ions and NH4+) and anions (halides, OH, CO32− and SO42−). The halide test above is its centrepiece; the sulfate test (acidified barium chloride) and the carbonate test (effervescence with acid) sit alongside it. Practical skills are examined on all three papers — see the required practicals page.

Precision points
  • Acidify with dilute nitric acid — examiner reports flag the missing acid step. Not HCl (adds chloride) and not H2SO4 (adds sulfate), which would ruin the test.
  • Learn the colours exactly: AgCl white, AgBr cream, AgI yellow. F gives no precipitate.
  • Ammonia distinguishes them: AgCl dissolves in dilute, AgBr only in concentrated, AgI in neither.
🧪 Exam-style questions
Q1 [1 mark]

In the test for a halide ion, dilute nitric acid is added before the silver nitrate solution. Why is the nitric acid added? Tick (✓) one box.

Q2 [1 mark]

State what is observed when silver nitrate solution is added to sodium fluoride solution.

Show answer

No change / colourless solution / no precipitate forms. 1 mark

Silver fluoride is soluble, so fluoride is the one halide that gives no precipitate.

Source: AQA A-Level Chemistry past papers.

Chlorine chemistry

Chlorine’s signature reactions are disproportionation — the same chlorine atoms are both oxidised and reduced, going from 0 to +1 (in the chlorate(I)) and 0 to −1 (in the chloride).

Key definition

Disproportionation is a reaction in which the same element is simultaneously oxidised and reduced.

Chlorine’s disproportionation reactions

With water (the basis of water treatment):

Cl2 + H2O ⇌ HCl + HClO

With cold, dilute sodium hydroxide (this makes bleach):

Cl2 + 2NaOH → NaCl + NaClO + H2O

In both, chlorine is 0 on the left, but ends up as +1 in the chlorate(I) (ClO) and −1 in the chloride (Cl) — that split is what “disproportionation” means. In bright sunlight, chlorine instead reacts with water to give chloride and oxygen: 2Cl2 + 2H2O → 4HCl + O2. That reaction is not disproportionation — here chlorine is only reduced (0 → −1), while it is the oxygen in the water that is oxidised (−2 → 0).

Cl₂ + H₂O ⇌ HCl + HClO +10−1 oxidation state of Cl Cl₂ · 0 oxidised · 0 → +1 reduced · 0 → −1 HClO · +1 HCl · −1 the same element goes both ways at once — that is disproportionation
Prove disproportionation with oxidation states: chlorine goes both ways from 0 — up to +1 and down to −1 — in a single reaction.
Chlorine in water treatment — a balance of risk

Chlorine is added to drinking water because the HClO / ClO it forms kills bacteria, preventing water-borne diseases such as cholera and typhoid. Chlorine is also toxic, and can form traces of chlorinated organic compounds — so society weighs the risks against the benefits, and judges that the health benefits of safe drinking water outweigh the toxic effects.

Precision points
  • Prove disproportionation with oxidation states. Examiner reports flag recall without the redox — show chlorine going 0 → +1 and 0 → −1.
  • Know the products of Cl2 + water: chloride and chlorate(I) (HCl + HClO), or chloride + oxygen in sunlight. OH and O3 are not products.
  • Water treatment answers need both sides: the benefit (kills bacteria) and the risk (toxic) — then the judgement that benefits outweigh risks.
🧪 Exam-style questions
Q1 [1 mark]

Which shows the major product(s) formed when chlorine reacts with cold, dilute, aqueous sodium hydroxide? Tick (✓) one box.

Q2 [1 mark]

Which species is never formed during the reactions of chlorine with water? Tick (✓) one box.

Q3 [2 marks]

Chlorine is used to treat drinking water even though it is toxic. Give one reason chlorine is added, and explain why its use is considered acceptable.

Show answer

Chlorine sterilises the water — it kills bacteria / microorganisms. 1 mark

The health benefits (preventing water-borne disease) outweigh the risk from its toxicity, and it is used only in small quantities. 1 mark

Source: AQA A-Level Chemistry past papers.

Capstone: the halogen toolkit

Group 7 is a set of trends that mirror each other, plus a handful of reactions worth knowing cold. Line the trends up first:

Down F → IDirectionWhy it matters
Electronegativitydecreasesbonding pair further from the nucleus
Boiling pointincreasesstronger van der Waals between bigger molecules
Oxidising power of the halogendecreasesdisplacement: a halogen displaces the halides below it
Reducing power of the halide ionincreasesconc. H2SO4: NaCl → HCl; NaBr → SO2; NaI → H2S

These trends also let you predict a halogen below iodine without ever having met it: it would be an even weaker oxidising agent (unable to displace the halide ions above it), its ion an even stronger reducing agent, and the element itself a darker solid with a higher boiling point — larger molecules mean stronger van der Waals forces.

The one exam skill that ties it together is choosing the right kind of equation. AQA asks for a full equation, an ionic equation or a half-equation, and they are not interchangeable. Take chlorine displacing bromide:

TypeChlorine + potassium bromide
Full equationCl2 + 2KBr → 2KCl + Br2
Ionic equationCl2 + 2Br → 2Cl + Br2
Half-equationsCl2 + 2e → 2Cl  and  2Br → Br2 + 2e

How to tell which is which: a full equation writes every substance out, potassium and all; an ionic equation drops the spectator ions (the K+) and keeps only the species that change; a half-equation shows just the oxidation or just the reduction on its own, with electrons added to balance the charge.

Read the command word, give exactly the equation asked for, and pin every observation to the right colour or gas — and Group 7 becomes one of the most dependable topics on Paper 1.

3.2.3 Group 7 — Quick-reference summary
  • Down F→I: electronegativity decreases (bonding pair further from nucleus/more shielded); boiling point increases (stronger van der Waals between larger molecules).
  • Oxidising power of the halogens decreases down the group: a halogen displaces the halide ions below it (Cl2 + 2Br → 2Cl + Br2). Colours: Br2 orange solution, I2 brown solution / grey-black solid.
  • Reducing power of the halide ions increases down the group (I strongest). With conc. H2SO4: NaCl → HCl only (no redox); NaBr → Br2 + SO2 (S +6→+4); NaI → I2 + S + H2S (S +6→−2).
  • Halide test: dilute HNO3 then AgNO3 → AgCl white, AgBr cream, AgI yellow (F none). Distinguish with ammonia: AgCl dissolves in dilute NH3, AgBr in conc. NH3, AgI insoluble.
  • Acidify with nitric acid (not HCl or H2SO4) to remove carbonate/hydroxide ions that would also precipitate.
  • Chlorine disproportionates (Cl 0 → +1 and 0 → −1): Cl2 + H2O ⇌ HCl + HClO (water treatment); Cl2 + 2NaOH → NaCl + NaClO + H2O (bleach). Chlorine’s health benefits in water treatment outweigh its toxicity.

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